Sample Volume And Preservation
Samples sent to HU Water Chemistry Laboratory should be in sufficient volume and be properly preserved. Please refer to following table (taken from Standard Methods) for details. Samples must reach the laboratory well before the maximum storage duration expires.

Parameter Minimum Sample Size(ml) Type of Sample Container Preservation Method Maximum Storage Duration Standard Method Number
Acidity 100 P,C Keep cool at 4°C 24 hour 402
Alkalinity 100 P,C Keep cool at 4°C 24 hour 403
Arsenic 100 P,C HNO3 to pH<2 6 month 404
BOD 1000 P,C Keep cool at 4°C 6 hour 507
Bromide 100 P,C Keep cool at 4°C 24 hour 406
COD 50 P,C H2SO4 to pH<2 7 day 508
Chloride 50 P,C None required 7 day 408
Chlorine (Residual) 50 P,C Keep cool at 4°C 24 hour 412
Color 50 P,C Keep cool at 4°C 24 hour 204
Cyanide 500 P,C Keep cool at 4°C NaOH to pH 12 24 hour 413
Dissolved Oxygen         402
    Probe 300 C In-situ measurement none  
    Winkler titration 300 C In-situ measurement none  
Fluoride 300 P,C Keep cool at 4°C 7 day 414
Hardness 100 P,C Keep cool at 4°C 7 day 309
Iodine 100 P,C Keep cool at 4°C 24 hour 416
MBAS 250 P,C Keep cool at 4°C 24 hour 512
Metals          
    Dissolved 200 P,C Filter in-situ, Add HNO3 to pH<2 6 month  
    Total Suspended 100   Filter in-situ, Add HNO3 to pH<2 6 month  
Mercury         315
    Dissolved 100 P,C Filter in-situ, Add HNO3 to pH<2 38 day (glass)  
        13 day (hard plastic)  
   Total 100 P,C Add HNO3 to pH<2 38 day (glass)  
        13 day (hard plastic)  
Nitrogen         417
    Ammonia 400 P,C Keep cool at 4°C H2SO4 to pH<2 24 hour 418
    Kjeldahl 500 P,C Keep cool at 4°C H2SO4 to pH<2 24 hour 421
    Nitrate 100 P,C Keep cool at 4°C H2SO4 to pH<2 24 hour 419
    Nitrite 50 P,C Keep cool at 4°C H2SO4 to pH<2 24 hour 420
NTA 50 P,C Keep cool at 4°C 24 hour -
Oil and grease 1000 C Keep cool at 4°C H2SO4 to pH<2 24 hour 502
Organic Carbon 25 P,C Keep cool at 4°C H2SO4 to pH<2 24 hour 506
pH 25 P,C Keep cool at 4°C Yerinde belirlenir 6 hour 424
Phenol 500 C Keep cool at 4°C H3PO4 to pH<4 1.0 g CuSO4/1- 24 hour 574
Phosphorus          
         Ortho-phosphate 50 P,C Filter in-situ,Keep cool at 4°C 24 hour 425
         dissolved          
     Hydrolized 50 P,C Keep cool at 4°C H2SO4 to pH<2 24 hour  
     Total 50 P,C Keep cool at 4°C 24 hour  
     Total dissolved 50 P,C Filter in-situ,Keep cool at 4°C 24 hour  
Residue         208
     Filtrable 100 P,C Keep cool at 4°C 7 day  
     Nonfiltrable 100 P,C Keep cool at 4°C 7 day  
    Total 100 P,C Keep cool at 4°C 7 day  
    Volatile 100 P,C Keep cool at 4°C 7 day  
Settleable Matter 1000 P,C None required 24 hour 208
Selenium 50 P,C Add H3PO4 to pH<4 6 month 318
Silica 50 P Keep cool at 4°C 7 day 426
Specific Conductivity 100 P,C Keep cool at 4°C 24 hour 205
Sülfate 50 P,C Keep cool at 4°C 7 day 427
Sulfide 50 P,C Add 2 ml zinc asetate 24 hour 428
Sulfite 50 P,C Keep cool at 4°C 24 hour 429
Temperature 1000 P,C In-situ measurement none 212
Odor 200 C Keep cool at 4°C 24 hour 206
Turbidity 100 P,C Keep cool at 4°C 7 day 214

P: Plastic(polyethylen or equivalent) sample container C: Glass sample container

Hacettepe University Water Chemistry Laboratory
Hacettepe Üniversitesi Jeoloji Mühendisliği Bölümü Hidrojeoloji Mühendisliği ABD. 06800 Beytepe/ANKARA
06800 Beytepe Ankara
Webmaster: Prof.Dr.Serdar Bayarı